N-Benzylaniline

Usetyenziso lweMveliso:

Ukumisela i-sulfonic acid, i-organic synthesis.

indlela yokuvelisa:

Isuka kwi-condensation ye-benzyl chloride kunye ne-aniline.Xuba kwaye uvuthulule i-sodium bicarbonate, amanzi kunye ne-aniline, ubushushu ukuya kwi-90-95 ° C, kwaye ngokukhawuleza wongeza i-benzyl chloride.Ukuphendula kwi-90-95 ° C kwi-3h.Ukupholisa kunye nesihluzo.I-filtrate yahlulwa, kwaye i-organic layer yahlanjwa nge-brine egcweleyo kwaye yomiswa phezu kwe-anhydrous sodium sulfate.Emva koko i-vacuum distillation, iqokelela i-81 ℃ (1.6kPa) iqhezu lokubuyisela i-aniline, i-170-190 ℃ (1.6kPa) ukupholisa kwamaqhezu, ukuqina ukufumana i-benzyl aniline.Inokuphinda ifakwe kwi-petroleum ether ngexesha lokuhlanjululwa.Isivuno singaphezulu kwama-80%.